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The complexes of the type [Hg(II)2Ln(2+)](6-n) (Ln = 2,2'-bipyridine; n = 3, n = 4, n = 6, n = 7) and [Cu(II)2Ln(2+)](6-n) (n = 2, 3; Ln = 2,2'-bipyridine; n = 4, 5, 6, 7) have been synthesized by reaction of the title compounds with the appropriate metal salts in methanol. The structures of the complexes were characterized by elemental analysis, conductometric and magnetic measurements, IR, NMR, and UV-vis spectroscopy, and cyclic voltammetry. The complexes have the tendency to form aggregate structures. The electrochemical properties of the complexes were investigated by cyclic voltammetry. The two-electron quasi-reversible oxidation waves at E1/2=1.13 (5), 1.05 (6), and 1.00 (7) V (vs. Ag/AgCl) are assigned to the oxidation of the pyridyl rings of the ligands. 0b46394aab